GCMS analysis results for sample AD27957, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27957.D Vial: 13 Acq On : 21 Dec 2001 3:06 am Operator: GALOS Sample : gems unknown 11/20 Inst • : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 1-Pentene, 2,4-dimethyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.68 0.48 ng/uL 209872 Chrysene-dl2 33.17

Hit# of 5 Tentative ID . MW MolForm CAS# Qual

1 1-Pentene, 2,4 dimethyl- 98 C7H14 002213-32-3 27 2 l - Hexene, 2,5-dimethyl - 112 C8H16 006975-92-4 27 3 1 -Heptene, 2-methyl- 112 C8H16 015870-10-7 27 4 Pentadecane, 8-methylene- 224 C16H32 055668-09-2 25 Abundance " ” Scan 2927 (31.683 min): 27957.D(-) m/z 56.10 100.00% 53

43 5000 ! 73 07 129 ■ ■ i ■ A..... rz—> I1'''n 20 40 IWX60 80 97 I ,117 II 185 207 267 285 »l l""l T ‘i ’ ’ • >TO"IEII"EE-0""III-‘"rT"‘IITr‘‘ITE‘IIIIr 100 120 140 160 180 200 220 240 260 280 m/z 31.40 31.60 31.80 32.00 57.10 59.08% Abundance #63263:1 -Pentene, 2,4-dimethyl- 55

43 5000 ' 1 1 1 ■ ■ ■ i --- 27 31.40 31.60 31.80 32.00 m/z 43.10 53.03% 70 83 98 ! ■ L । । < > i । > , ________________________________________________ miz- 20 40 60 80 100 120 140 160 180 200 220 240 260 280 [Abundance #64038’ 1 -Hexene. 2,5-dimethyl- 56

41 ---AAA 31.40 31.60 31.80 32.00 5000 m/z 41.10 44.50% 27 ; f 69 ! 112

miz-> 20 40 60 80 100 120 140 160 180 ’266 220 ' 240 260 280 Abundance #64030:1-Heptene, 2-methyl- ■ AAA- , । , , ■ M A4AA 56 31.40 31.60 31.80 32.00 m/ Z 55.10 35.49% 5000 - 41

27 69

-p-m-p-r i1' . 497 112L.... .. ...... TTT 4 ALLA AM—— miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 31.40 31.60 31.80 32.00

27957.D NP112701.M Fri Dec 21 10:07:28 2001 Page 7

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