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GCMS Method 508 calibration data sheet, Nov 2001

Machine-extracted title · confidence 100%

Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.

NYC-WTC_000033886–000033901

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

Quantitation Report

Data File : M:\INSTRU~1\2 09\DATA\NOV26 01\LBA.D Vial: 9 Acq On : 26 Nov 2001 6:31 pm Operator: 209 GALOS Sample : 11/20 lab bik scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 27 12:32 2001 Quant Results File: GCMS1126.RES

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration . Abundance”' TIC: LBA.D 1 4000000

: 3800000

> 3600000 ! t 9 | 3400000

3200000

: 3000000 2

I 1 2800000 i 2600000 §

? 2400000 CM

I ■ 2200000

2000000 e 1800000

i 1600000 I | 1400000

1200000

1000000

800000 g 3 2 600000 a s o 3 C I 400000 18 5 200000

! Time-> 0- —P.P i — - 1 ,4 — — . i - fi — । n —+ i I ' ' , ' I ’ ' • ' i ' ' ' ' I ’ frT 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00 42.00 44.00 46.00

LBA.D GCMS1126.M Tue Jan 08 09:40:57 2002 Page 3

NYC-WTC_000033889

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NYC-WTC_000033889Source: NYC Law Department, mirrored locally

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GCMS comments for sample AD28149, Nov 2001 · Box DEP Box 21

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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

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