Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
NYC-WTC_000033886–000033901Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : M:\INSTRU-1\209\DATA\NOV2 6 01\LBA.D Vial: 9 Acq On : 26 Nov 2001 6:31 pm Operator: 209 GALOS Sample : 11/20 lab bik scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 27 12:32 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth : NP103001
Compound R.T. Qlon Response Cone Unit Qvalue
29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 0.00 162 0 N.D. 31) Dimethylphthalate 19.99 163 355 N.D. 32) 2,6-Dinitrotoluene 0.00 165 0 N.D. 33) Acenaphthylene 0.00 152 0 N.D. 34) Ac enapht hene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 21.03 165 680 N.D. 38) Diethylphthalate 22.09 149 1993 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 22.70 77 199 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. , 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.05 178 1478 N.D. 49) Anthracene 25.20 178 1044 N.D. 50) Di-n-butylphthalate 27.00 149 15058 N.D. 51) Fluoranthene 28.68 202 2612 N.D. 54) Pyrene 29.35 202 2704 N.D. 55) Butylbenzylphthalate 31.51 149 9516 N.D. 56) Benzo(a)anthracene 32.98 228 15087 N.D. 57) Bis(2-ethylhexyl)phthalate 33.31 149 54976 0.60 ug/1 98 58) Chrysene 33.10 228 15990 N.D. 60) Di-n-Octylphthalate 35.04 149 37796 0.26 ug/1 # 88 61) Benzo(b)fluoranthene 36.06 252 12301 N.D. 62) Benzo(k)fluoranthene 36.06 252 10873 N.D. 63) Benzo(a)pyrene 36.95 252 9986 N.D. 64) Indeno(1,2,3-cd)pyrene 40.84 276 5584 N.D. 65) Dibenz(a,h)anthracene 40.89 278 3690 N.D. 66) Benzo(g,h,i)perylene 41.91 276 7192 N.D.
(#) = qualifier out of range (m) = manual integration LBA.D GCMS1126.M Tue Jan 08 09:40:46 2002 Page 2
NYC-WTC_000033888
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Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
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Header page for a gas chromatography-mass spectrometry scan file related to environmental testing at the World Trade Center site.
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Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
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Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
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Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
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Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
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Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
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Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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GCMS blank analysis report for sample AE08209 listing volatile organic compounds from April 2002.
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Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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