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GCMS comments for sample AD28155, Nov 2001

Machine-extracted title · confidence 100%

Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.

NYC-WTC_000033834–000033846

Folder label: “GCMS X 11/20/01 A 11/26/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2 601\28155.D Vial: 11 Acq On : 26 Nov 2001 8:29 pm Operator: 209 GALOS Sample 11/20 scan Inst : GC/MS 209 Mise s Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 27 12:54 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. QIon Response Cone Unit Qvalue

33) Acenaphthylene 0.00 152 0 N.D. 34) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 21.05 165 183 N.D. 38) Diethylphthalate 22.09 149 888 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. .41) Azobezen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.07 178 394 N.D. 4 9) Anthracene 25.07 178 3 94 N.D. 50) Di-n-butylphthalate 27.01 149 6119 N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 29.36 202 261 N.D. 55) Butylbenzylphthalate 31.51 149 946 N.D. 56) Benzo(a)anthracene 33.10 228 2416 N.D. 57) Bis(2-ethylhexyl)phthalate 33.30 149 25353 0.35 ug/1 92 58) Chrysene 33.10 228 2416 N.D. 60) Di-n-Octylphthalate 35.05 149 5224 N.D. 61) Benzo(b)fluoranthene 36.12 252 6266 N.D. 62) Benzo(k)fluoranthene 36.12 252 9634 N.D. 63) Benzo(a)pyrene 36.95 252 4027 N.D. 64) Indeno(l,2,3-cd)pyrene 40.84 276 4250 N.D. 65) Dibenz(a,h)anthracene 40.87 278 3211 N.D. 66) Benzo(g,h,i)perylene 41.91 276 5062 N.D.

(#) = qualifier out of range (m) = manual integration 29155.D GCMS1126.M Tue Nov 27 12:55:56 2001 Page 2

NYC-WTC_000033837

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NYC-WTC_000033837Source: NYC Law Department, mirrored locally

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Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

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