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GCMS analysis results for sample AD28434, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD28434 conducted between November 21 and 26, 2001.

NYC-WTC_000034302–000034310

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2901\28434.D Vial: 26 Acq On : 29 Nov 2001 12:36 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 29 15:33 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. QIon Response Cone Unit Qvalue 3 3) Acenaphthylene 0.00 152 0 N.D. 34) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 20.87 165 447 " N.D. 3 8) Diethylphthalate 22.10 149 355 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.05 178 424 N.D. 49) Anthracene 25.05 178 424 - N.D. 50) Di-n-butylphthalate 27.00 149 29952 N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 0.00 149 0 N.D. 56) Benzo(a)anthracene 33.03 228 2991 / N.D. 57) Bis(2-ethylhexyl)phthalate 33.30 149 1391 N.D. 58) Chrysene 33.03 228 2991 N.D. 60) Di-n-Octylphthalate 0.00 149 0 N.D. 61) Benzo(b)fluoranthene 36.13 252 638 N.D. 62) Benzo(k)fluoranthene 36.13 252 436 N.D. 63) Benzo(a)pyrene 37.11 252 2342 N.D. 64) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28434.D GCMS1126.M Thu Nov 29 15:33:28 2001 Page 2

NYC-WTC_000034305

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NYC-WTC_000034305Source: NYC Law Department, mirrored locally

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