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GCMS analysis results for sample AD28145, Nov 2001

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Laboratory report detailing GCMS analysis of sample AD28145 conducted on November 29, 2001, noting unknown compounds.

NYC-WTC_000033731–000033741

Folder label: “GCMS X 11/20/01 A 11/26/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2601\28145.D Vial: 10 Acq On : 26 Nov 2001 7:29 pm Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplrs 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 27 12:51 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. QIon Response Cone Unit Qvalue

33) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 21.00 165 112 N.D. 38) Diethylphthalate 22.09 149 877 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.05 178 362 N.D. 49) Anthracene 25.05 178 362 N.D. 50) Di'-n-butylphthalate 27.00 149 10729 N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.53 149 429/ N.D. 56) Benzo(a)anthracene 33.03 228 5011/, N.D. 57) Bis(2-ethylhexyl)phthalate 33.30 149 12151 N.D. 58) Chrysene 33.10 228 3038 N.D. 60) Di-n-Octylphthalate 35.04 149 N.D. 61) Benzo(b)fluoranthene 36.06 252 3841 N.D. 62) Benzo(k)fluoranthene 36.13 252 57 N.D. 63) Benzo(a)pyrene 36.95 252 2968 N.D. 64) Indeno(1,2,3-cd)pyrene 40.86 276 N.D. 65) Dibenz(a,h)anthracene 0.00 278 >—0 N.D. 66) Benzo (g, h, i)perylene 41.93 276 128 N.D.

(#) = qualifier out of range (m) = manual integration 28145.D GCMS1126.M Tue Nov 27 12:52:23 2001 Page 2

NYC-WTC_000033734

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NYC-WTC_000033734Source: NYC Law Department, mirrored locally

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GCMS comments for sample AD28151, Nov 2001 · Box DEP Box 21

NYC-WTC_000033789

Analytical commentary for sample AD28151 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

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