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GCMS blank analysis results for sample AD28143, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.

NYC-WTC_000033707–000033722

Folder label: “GCMS X 11/20/01 A 11/26/01

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Scanned page image, NYC-WTC_000033709
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\NOV2601\LBA.D Vial: 9 Acq On 26 Nov 2001 6:31 pm Operator: 209 GALOS Sample : 11/20 lab blk scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 27 12:32 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 0.00 152 0 N.D. 34) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 21.03 165 680 N.D. 38) Diethylphthalate 22.09 149 1993 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 22.70 77 199 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 243 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.05 178 1478 N.D. 49) Anthracene 25.20 178 1044 N.D. 50) Di-n-butylphthalate 27.00 149 15058 N.D. 51) Fluoranthene 28.68 202 2612 N.D. 54) Pyrene 29.35 202 2704 N.D. 55) Butylbenzylphthalate 31.51 149 9516 N.D. 56) Benzo(a)anthracene 32.9 228 15087 N.D. 57) Bis(2-ethylhexyl)phthalate 33.31 149 54976 0.60 ug/1 98 58) Chrysene 33.10 228 15990 N.D. 60) Di-n-Octylphthalate 35.04 149 37796 0.26 ug/1 # 88 61) Benzo(b)fluoranthene 36.06 252 12301 N.D. 62) Benzo(k)fluoranthene 36.06 252 10873 N.D. 63) Benzo(a)pyrene 36.95 252 9986 N.D. 64) Indeno(1,2,3-cd)pyrene 40.84 276 5584 N.D. 65) Dibenz(a,h)anthracene 40.89 278 3690 N.D. 66) Benzo(g,h,i)perylene 41.91 276 7192 N.D.

(#) = qualifier out of range (m) = manual integration LBA.D GCMS1126.M Tue NOV 27 12:39:23 2001 Page 2

NYC-WTC_000033709

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NYC-WTC_000033709Source: NYC Law Department, mirrored locally

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GCMS comments for sample AD28157, Nov 2001 · Box DEP Box 21

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GCMS comments for sample AD28149, Nov 2001 · Box DEP Box 21

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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

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