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GCMS comments for sample AD28151, Nov 2001

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Analytical commentary for sample AD28151 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

NYC-WTC_000033789–000033799

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\NOV2 601\28151.D Vial: 18 Acq On 27 Nov 2001 3:19 am Operator: 209 GALOS Sample 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 28 7:53 2001 Quant Results Files GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue NOV 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 0.00 152 0 N.D. 34) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 20.92 165 374 N.D. 38) Diethylphthalate 22.10 149 332 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 4 7) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.00 178 597 N.D. 49) Anthracene 25.00 178 597 N.D. 50) Di-n-butylphthalate 27.00 149 3504 N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 0.00 149 0 N.D. 56) Benzo(a)anthracene 33.02 228 2255 N.D. 57) Bis(2-ethylhexyl)phthalate 33.31 149 7019 N.D. 58) Chrysene 33.10 228 391 N.D. 60) Di-n-Octylphthalate 35.03 149 791 N.D. 61) Benzo(b)fluoranthene 36.09 252 727 N.D. 62) Benzo(k)fluoranthene 36.14 252 1554 N.D. 63) Benzo(a)pyrene 37.11 252 2197 N.D. 64) Indeno(1, 2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 41.89 276 560 N.D.

(#) = qualifier out of range (m) = manual integration 28151.D GCMS1126.M Wed Nov 28 07:55:13 2001 Page 2

NYC-WTC_000033792

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NYC-WTC_000033792Source: NYC Law Department, mirrored locally

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