GCMS analysis results for sample AD27548, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC13O1\27548.D Vial: 7 Acq On 13 Dec 2001 3:50 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 Cyclohexane, octyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

10.83 0.66 ng/uL 210324 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, octyl- 196 C14H28 001795-15-9 38 2 2-Pentene, 4,4-dimethyl- 98 C7H14 026232-98-4 35 3 7-Oxabicyclo[4.1.0]heptane 98 C6H10O 000286-20-4 28 4 Cyclohexane, hexyl- 168 C12H24 ____ 004292-75-5 25 Abundance Scan 653 (10.830 min): 27548.D (-) m/z 43.10 100.00% 43 83 / 55 5000 71 — 10.40 10.60 10.80 11.00 11.20 100 „ 0110011 T T । T--- 1‘ —100000n0‘UCOUTTTTTTT T’T’TTITTTT m/z 83.05 67.96% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #69529: Cyclohexane, octyl- 83

5000 55 10.40 10.60 10.80 11.00 11.20 67 m/ Z 55.10 55.77%

m/z-> 30 40 42 50 60 70 80 +9 112 T‘-rr-rp-TTTTUBTTUUTT I"1' I 90 100 110 120 130 140 150 160 170 180 190 200 196 TTT Abundance #1340: 2-Pentene. 4,4-dimethyl- 55 83 X A I ' ' I T IT 10.40 10.60 10.80 11.00 11.20 5000 m/z 71.05 31.58% 98 42 67 1 . I < "T’T1 i" " i II‘IEIIETTTT‘‘IIT‘ID"VTTBT‘TIETTTETTTTTTTTTT ' i ‘ " i " " i1 ‘ITT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #1310: 7-Oxabicyclo[4.1.0]heptane A ’ ‘ I - ■ i ' ' 41 83 10.40 10.60 10.80 11.00 11.20 m/ Z 58.10 28.63% 55 5000 70 98

m/z-> i' ‘ Id’ 30 40 ■ ■ i''

50 - 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ItT A..... . 10.40 10.60 10.80 11.00 11.20

27548.D NP112701.M Fri Dec 14 12:56:15 2001 Page 7

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