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GCMS analysis results for sample AD27769, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD27769 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033388–000033402

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC19 01\27769.D Vial: 12 Acq On : 20 Dec 2001 5:57 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.483 173 179 184 rBV 118656 225835 2.88% 0.568% 2 6.584 184 190 199 rW 212898 463673 5.92% 1.166% 3 6.722 199 205 210 rW2 124403 261057 3.33% 0.656% 4 6.832 211 217 225 rBV 174299 340018 4.34% 0.855% 5 7.776 316 320 324 rBV 131459 250181 3.19% 0.629%

6 7.850 324 328 340 rVB 407856 831265 10.61% 2.090% 7 11.875 761 767 775 rBV 2838935 5967087 76.14% 15.003% 8 15.479 1153 1160 1177 rBV 3198134 7836506 100.00% 19.704% 9 20.761 1727 1736 1752 rBV 3309246 7620737 97.25% 19.161% 10 25.172 2207 2217 2227 rBV2 3243730 7148637 91.22% 17.974%

11 25.309 2227 2232 2238 rVB 35537 83389 1.06% 0.210% 12 33.177 3082 3090 3101 rVB2 2324655 5484500 69.99% 13.790% 13 37.258 3528 3535 3544 rVB2 1199100 3258534 41.58% 8.193%

Sum of corrected areas: 39771419

27769.D NP112701.M Thu Dec 20 11:47:06 2001

NYC-WTC_000033394

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NYC-WTC_000033394Source: NYC Law Department, mirrored locally

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