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GCMS analysis results for sample AD27767, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27767 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033358–000033372

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27767.D Vial: 10 Acq On : 20 Dec 2001 4:08 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method . : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.480 174 179 185 rBV 126317 252218 3.14% 0.597% 2 6.581 185 190 194 rW 235668 436067 5.42% 1.032% 3 6.709 200 204 212 rW 148224 267775 3.33% 0.634% 4 6.819 212 216 224 rVB 180023 355754 4.42% 0.842% 5 7.773 315 320 324 rBV 270130 489817 6.09% 1.160%

6 7.846 324 328 340 rVB 893974 1736924 21.60% 4.112% 7 11.872 761 767 777 rW 2977475 6094757 75.79% 14.428% 8 15.485 1154 1161 1179 rBV 3390290 8042097 100.00% 19.038% 9 20.758 1728 1736 1750 rBV 3364782 7817007 97.20% 18.505% 10 25.178 2206 2218 2228 rBV2 3240218 7399972 92.02% 17.518%

11 33.174 3083 3090 3099 rBV2 2480383 5767611 71.72% 13.654% 12 37.264 3528 3536 3545 rVB2 1319281 3582559 44.55% 8.481%

Sum of corrected areas: 42242558

27767.D NP112701.M Thu Dec 20 11:45:51 2001

NYC-WTC_000033364

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NYC-WTC_000033364Source: NYC Law Department, mirrored locally

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