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GCMS analysis results for sample AD27639, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27639 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033221–000033246

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1801\27639.D Vial: 3 Acq Oil 18 Dec 2001 5:44 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.043 11 22 27 rBV 82912 251226 4.35% 0.681% 2 5.116 27 30 34 rW 266347 457606 7.92% 1.240% 3 5.180 34 37 53 rVB 388989 849199 14.69% 2.301% 4 5.611 81 84 87 rW 37881 72284 1.25% 0.196% 5 5.666 87 90 102 rVB 61199 134540 2.33% 0.365%

6 6.115 135 139 152 rBV 229554 537339 9.29% 1.456% 7 6.464 173 177 185 rBV 115032 243378 4.21% 0.660% 8 6.565 185 188 199 rVB 136189 301377 5.21% 0.817% 9 6.693 199 202 211 rBV 129338 310183 5.37% 0.841% 10 6.812 211 215 220 rBV2 105804 225996 3.91% 0.612%

11 6.922 223 227 232 rVB 39717 78320 1.35% 0.212% 12 7.023 235 238 243 rVB 39822 73971 1.28% 0.200% 13 7.179 246 255 259 rBV 1683566 3820225 .66.08% 10.353% 14 7.766 315 319 323 rBV 101748 189589 3.28% 0.514% 15 7.830 323 326 339 rVB 1038713 1984264 34.32% 5.378%

16 9.334 486 490 505 rBV 209127 379499 6.56% 1.028% 17 10.297 590 595 605 rBV 526030 1048073 18.13% 2.840% 18 10.508 613 618 625 rBV 425205 793166 13.72% 2.150% 19 10.829 649 653 659 rVB 72258 141345 2.44% 0.383% 20 11.865 761 766 774 rBV 2210086 4580163 79.22% 12.413%

21 15.478 1154 1160 1174 rBV 2824110 5781339 100.00% 15.668% 22 20.751 1728 1735 1751 rBV 2614891 5360098 92.71% 14.527% 23 25.153 2209 2215 2227 rBV2 2045020 4474731 77.40% 12.127% 24 33.149 3081 3087 3102 rVB2 1213643 2689763 46.52% 7.290% 25 37.239 3526 3533 3546 rBV2 789551 2120848 36.68% 5.748%

Sum of corrected areas: 36898522

NYC-WTC_000033227

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NYC-WTC_000033227Source: NYC Law Department, mirrored locally

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