GCMS analysis results for sample AD27638, Jan 2002

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Library Search Compound Report

Data File C : \HPCHEM\ 1 \DATA\DEC19 01\27638.D Vial: 21 Acq On 20 Dec 2001 4:09 pm Operator: GALOS Sample gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.48 1.01 ng/uL 289356 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexa: ne 100 C6H120 000589-38-8 91 2 3-Hex» one 100 C6H120 000589-38-8 91 3 3-He: none 100 C6H120 000589-38-8 87 4 3-P tanone, 2-methyl- 100 C6H120 000565-69-5 47 Abundance Scan 178 (6.476 min): 27638.D (-) m/z 43.10 100.00% 43 57

71 5000 100 1 — -P 39

m/z-> r • • • i ”111 Ml +85 53, 1TTTTTTTTT HDTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 i * * ‘' i p m/z 6.20 57.10 6.40 6.60 6.80 91.57% Abundance #63358:3-Hexanone 43

U 57

71 5000 6.20 6.40 6.60 6.80 100 m/z 71.05 53.2 9% 85 TIT TT I' ‘ " I ‘ ' I T’ I ‘' TTT i1 TTT TTTT Tp r m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance

29 #63357: 3-Hexanone 43 57 ........................ — 6.20 6.40 A 6.60 6.80 5000 71 m/z 100.15 27.14% 100

i "111" ■1111 ■ ■ i m*mp ■ ■ i ■1" r ■1 ■ i ■ ■" r ■'111" ■ i" " i" ■ ■ i •" ■ i1 ’"' i' ’" i ’ 85 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone ■ ■ । ■ > ■ ■ । 43 57 6.20 6.40 6.60 6.80 m/z 41.10 22.83%

NWL 29 71 5000 100 85 L/z~> TIp—r i ■ ■ ■ • i ■ ■ ■ ■ i • TTTTTTTTTTT I" " i " " I 11 " i" " i' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

27638.D NP112701.M Fri Dec 21 09:21:01 2001 Page 1

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