GCMS analysis results for sample AD26680, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC04 01\2 668 0 . D Vial: 3 Acq On 4 Dec 2001 12:38 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Oxirane, 2-methyl-3-propyl-, c Concentration Rank II

R.T. EstConc Area Relative to ISTD R.T.

5.65 0.46 ng/uL 123577 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2-methyl-3-propyl- , cis- 100 C6H120 006124-90-9 25 2 Undecane, 2,4-dimethyl- 184 C13H28 017312-80-0 10 3 2-Buten-1-ol 72 C4H80 006117-91-5 9 4 Hydrazine, 2-propenyl-______________ 72 C3H8N2 _______ 007422-78-8 9 Abundance Scan 88 (5.652 min): 26680.D (-) m/z 41.10 100.00% 41 57 85 5000-

1 „ll 71 ——4 5.40 5.60 5.80 6.00 ' TTT । । । । । । Tt ■ i ■ ' ' ' i ' i ■ ■ ' ■ i ■ ’ ' ■ i ■ ■ • ■ i ■ ■ ■ ' i ■ ■ ' ■ i ' ‘ ■ i ■ ■ ' ■ i m/z 45.10 83.80% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- i 43

57 5000 71 85 1— A 5.40 5.60 •I----- 1A 5.80 6.00 m/ z 4 3.05 71.20%

1 — j 100 1 ................ ■ i ■ ■ ' i ' ■ ■ ' i । m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #69023: Undecane. 2,4-dimethyl- i 43 i 57 5.40 5.60 5.80 6.00 85 5000 m/z 57.10 69.09% 71

................ I ' ' ‘' I ' _______________ I. 99 126 141 ' I ' ■ ' ' I ' ' ' ' I ' ' ' ' I ' ' ‘ ' I ' mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #62478: 2-Buten-1-ol i 57 5.40 5.60 5.80 6.00 m/z 85.05 61.19% 5000 72 31 42

|1' — 48, Ji, — — ' ' i ' ' ' ' i ' ' ' ' i ' ' ' ' I ' ' ' 1 I 1 ri "''I "’IrT’ 1 1 1 I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 5.40 5.60 5.80 6.00

26680.D NP112701.M Fri Dec 07 13:11:32 2001 Page 4

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