GCMS calibration data for TCLP analysis dated December 7, 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 7 01\LB.D Vial: 2 Acq On 7 Dec 2001 7:01 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Propanamide, N-acetyl- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

9.34 0.49 ng/uL 150415 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanamide , N-acetyl- 115 C5H9NO2 019264-34-7 33 2 Acetic acid 60 C2H402 000064-19-7 9 3 Ethylamine 45 C2H7N 000075-04-7 5 4 Acetic acid 60 C2H402 000064-19-7 5 Abundance Scan 491 (9.342 min): LB.D (-) m/z 43.1.0 100.00% i 43

5000 TIIm > । , -j-s-n-T-f . . . . , r . . . । . 60 9.00 9.20 9.40 9.60 78 87 * m/z 45.00 25.92% miz-> 10 20 30 40 "sb" 60 70 80 90 100 110 120 Abundance #64232: Propanamide, N-acetyl- 43

5000 —44— MWWA4 29 9.00 9.20 9.40 9.60 57 m/z 44.0,0 24.51%

miz-> Abundance — TIT 10 20 30 — 40 —+—— 50 60 70 #116; Acetic acid 73

80 87 ■ i • ■ ■ ■ । 90 115 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i' ■ 100 110 120 40 TTI TB—n—BmnT । । । 9.00 9.20 9.40 9.60 5000 60 m/ z 60.00 15.22% 15 (

> . • i •' 25 31 r-]-r m-r-m-rT BBB . r t . 1113 . . . . । ■ i ■ • ‘ ■ i ■ miz-? 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #42: Ethylamine ■ ■ i ■ ■ ■ ■ i • • ■ i | i । | ' 30 9.00 9.20 9.40 9.60 m/z 61.00 12.57% 5000 44 15 1

m/z—> —l 20 1030I , . 38, . .................................... .............. 40 50 60 70 1 1 ' 1 r1 80 90 1 ' i 1 1 1 1 I 1 1 1 1 I 1 11 1 1 1 1 ‘ ■ i • ‘ 1 ■ i 1 • ■ ■ i ■ • ' ■ i ■ ■ 100 110 120 9.00" 9.20 9.40 9.60

LB.D NP112701.M Thu Dec 13 11:28:42 2001 Page 11

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