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GCMS Analysis Report for Sample AD26388, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.

NYC-WTC_000031452–000031472

Folder label: “GCMS X 11/5/01 A 12/1/01

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Scanned page image, NYC-WTC_000031468
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26388.D vial: 14 Acq On : 1 Dec 2001 12:02 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Acetic acid Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 9.36 0.64 ng/uL 281259 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid / 60 C2H402 000064-19-7 9 2 Propanamide, N-acetyl- 115 C5H9NO2 019264-34-7 9 3 Ethylamine / 45 C2H7N 000075-04-7 5 4 Monomethylnitrosamine 60 CH4N20 000000-00-0 5 Abundance Scan 492 (9,357 min): 26388. D (-) m/z 43.00 100.00% 43

5000

—5 61 78 87 TT TTur fumpuu—I J 1 ‘ • I ' ' ‘ ‘ I ' ' ‘ rlerr/t r , > i IT 9.00 m/z 9.20 45.00 9.40 9.60 21.46% 9.80

m- 10 20 30 40 50 60 70 80 90 100 110 120 i

Abundance #116: Acetic acid 43

5000 60 -1.j .... t । . 9.00 9.20 9.40 9.60 9.80 15 m/z 61.10 17.95%

mz—> . 1—2.3.J 10 20 30 40 60 70 18090100110 120 Abundance #64232: Propanamide, N-acetyl- 43 9.00 9.20 9.40 9.60 9.80 5000 m/z 44.00 16.87% 29 57 73 —r TTT I 4 ■ ' I " _]......87......... T i | ’ 1 | * * * * | * * * 'I * * 115 T TTII I J I T m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #42: Ethylamine 33 9.00 9.20 9.40 9.60 9.80 m/z 60.10 12.81% 5000

44 15 i L, L. 38, | |_________________________________________ 111111r i 1 11 * j«■ ' ■ 1 i 1 1 ‘ i ■ ‘ ' i ‘ ' 1 i ‘ ' 1 i ■ ' ' ■ i ■ ■ ‘ • i 1 ' ' ■ i ‘ ‘ ‘ i ■ 1 ‘ I ' 1 • ‘ I « ‘ * 1 * m/z—> 10 20 30I 40 50 60 70 80 90 100 110 120 9.00 9.20 9.40 9.60 9.80

26388.D NP112701.M Tue Dec 04 10:40:26 2001 Page 11

NYC-WTC_000031468

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NYC-WTC_000031468Source: NYC Law Department, mirrored locally

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