GCMS comments for sample AD26710 detecting phthalate and tetrachloroethane

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 5 01\26710.D Vial: 4 Acq On 5 Dec 2001 11:29 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Acetic acid Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

9.36 0.42 ng/uL 142274 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid 60 C2H402 000064-19-7 9 2 Ethylamine 45 C2H7N 000075-04-7 7 3 Monometh nitrosamine 60 CH4N20 000000-00-0 7 4 Acetic cid 60 C2H402 000064-19-7 4 Abundance 7 Scan 493 9.362 min): 2671O.D(-) m/ z 43.LO 100.00% 43

5000-

61 9.00 9.20 9.40 9.60 9.80

mZ-? 5 ' r ■ ■' r r ' ■ ■ r ■ ■' I ■ ■ ■ ■ i —Qlll 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ■ v' > > 11 78 । 8/ ।. i. TTir m/ z 45.00 23.98% ‘Abundance #116: Acetic acid 4(3

5000 A AAYWAA 4 AL — 60 9.00 9.20 9.40 9.60 9.80 15 m/Z 4 4.0p 18.26% —— 26 31 .46 ' 11 " 111 TT’B I'1" I i ■ • • 'i ■'111" ■' TT ■111 TTTTTTT m/z-> 5 1C 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #42: Ethylamine 30

9.00 9.20 9.40 9.60 9.80 5000 m/ Z 61.00 15.84% 44 15 27 3841 I [ I HI | I .11 | II I I | I I I ! | I > i I | I I'rl' i " " i''" i" " i T‘‘tt1rwTEIIIUETOTTTTTTTTTr m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #110: Monomethylnitrosamine ... L JA / ) 43 9.00 9.20 9.40 9.60 9.80 8000- m/z 60.00 3.85% 30

6000

4000-1 m/z--> 5 10 15 TPTH " i " " i'' I " " 11 '-nyrr 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 60 TTT’TT1O‘O011——0100011111710T 9.00 9.20 L 9.40 9.60 9.80

26710.D NP112701.M Fri Dec 07 13:14:06 2001 Page 4

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