Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.
NYC-WTC_000031129–000031158Folder label: “GCMS X 11/2/01 A 12/1/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
° Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC0401\26205.D Vial: 68 Acq On : 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc Multipir: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 4 11:14 2001 Quant Results File: NP112601.RES
Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 09:03:50 2001 Response via : Initial Calibration DataAcq Meth : NP112601
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.70 152 1045274 20.00 ug/1 0.00 19) Naphthalene-d8 15.31 136 4025693 20.00 ug/1 0.00 31) Acenaphthene-d10 20.59 164 1931896 20.00 ug/1 0.01 49) Phenanthrene-d10 25.01 188 2727682 20.00 ug/l 0.01 59) Chrysene-d12 33.04 240 1755774 20.00 ug/1 0.00 68) Perylene-d12 37.13 264 1292798 20.00 ug/1 0.01
System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/l Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 10.78 99 177 0.00 ug/l -0.16 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.69 132 1022 0.01 ug/l 0.49 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.23 152 12970 0.30 ug/l 0.01 Spiked Amount 50.000 Recovery = 0.60% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/l Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.73 172 4567 0.04 ug/1 0.15 Spiked Amount 50.000 Recovery = 0.08% 33) 2,4,6-Tribromophenol 22.81 330 498 0.04 ug/1 -0.19 Spiked Amount 75.000 Recovery = 0.05% 62) Terphenyl-d14 29.91 244 430 0.00 ug/l 0.00 Spiked Amount 50.000 Recovery = 0.00%
Target Compounds Qvalue •2) Pyridine 5.65 79 1190 N.D. 3) N-nitroso-dimethyl amine 5.19 74 635 N.D. 8) Phenol 11.06 94 783 N.D. 9) bis(2-Chloroethyl)ether 10.99 93 1577 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(l-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 13.44 77 189 N.D. 22) Isophorone 0.00 82 0 N.D. -------------------------------------------------------------------------- (#) =. qualifier out of range (m) = manual integration 26205.D NP112601.M Tue Dec 04 15:53:18 2001 Page 1
NYC-WTC 000031132
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NYC-WTC_000031088
Gas chromatography-mass spectrometry analysis of environmental sample AD26202 conducted Dec 5, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068413
Laboratory report documenting GCMS analysis of sample AD24431 conducted on November 7-9, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088905
Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087274
Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069215
Laboratory report documenting GCMS analysis of sample AD25038 conducted on November 19, 2001, noting violations and unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000030966
Single-page GCMS document identifier from the Environmental Protection Department archive covering late 2001 testing records.
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Laboratory report documenting GCMS analysis of sample AD26129 conducted on December 3, 2001.
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Laboratory report documenting GCMS analysis of sample AD26128 conducted on December 3, 2001.
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NYC-WTC_000030992
Laboratory report documenting GCMS analysis of sample AD26130 conducted on December 3, 2001.
Filed in the same folder