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GCMS analysis results for sample AD26203, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26203 with unidentified compounds detected.

NYC-WTC_000031118–000031128

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\DEC0401\26204.D Vial: 69 Acq On : 4 Dec 2001 11:24 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 4 12:15 2001 Quant Results Files NP112601.RES Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 09:03:50 2001 Response via : Initial Calibration DataAcq Meth : NP112601

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.70 152 1052296 20.00 ug/1 0.00 19) Naphthalene-d8 15.31 136 4001315 20.00 ug/1 0.00 31) Acenaphthene-diO 20.59 164 1903097 20.00 ug/1 0.01 49) Phenanthrene-diO 25.01 188 2656953 20.00 ug/1 0.01 59) Chrysene-dl2 33.04 240 1655175 20.00 ug/1 0.00 68) Perylene-dl2 37.13 264 1175969 20.00 ug/1 0.01 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.70 132 847 0.01 ug/1 0.50 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.22 152 9932 0.22 ug/1 0.00 Spiked Amount 50.000 Recovery = 0.44% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.74 172 4664 0.04 ug/1 0.15 Spiked Amount 50.000 Recovery 0.08% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2' -oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 13.23 77 187 N.D. 22) Isophorone 0.00 82 0 N.D.

(#) = qualifier out of range (m) = manual integration 26204.D NP112601.M Tue Dec 04 15:50:33 2001 Page 1

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NYC-WTC_000031120Source: NYC Law Department, mirrored locally

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