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GCMS analysis results for sample AD26130, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD26130 conducted on December 3, 2001.

NYC-WTC_000030992–000031002

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C: \HPCHEM \ 1 \DATA\NOV3 001\26130.D Vial: 67 Acq On : 1 Dec 2001 7:18 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 1 8:07 2001 Quant Results File: NP112601.RES Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 09:03:50 2001 Response via : Initial Calibration DataAcq Meth : NP112601

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.70 152 740337 20.00' ug/1 0.00 19) Naphthalene-d8 15.31 136 2834905 20.00 ug/1 0.00 31) Acenaphthene-dl0 20.58 164 1311397 20.00 ug/1 0.00 49) Phenanthrene-dl0 25.00 188 1767433 20.00 ug/1 0.00 59) Chrysene-dl2 33.03 240 1072253 20.00 ug/1 0.00 68) Perylene-dl2 37.13 264 748948 20.00 ug/1 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.70 132 874 0.02 ug/1 0.49 Spiked Amount 75.000 Recovery = 0.03% 7) 1,2-Dichlorobenzene-d4 12.22 152 9050 0.29 ug/1 0.00 Spiked Amount 50.000 Recovery = 0.58% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2“Fluorobiphenyl 18.73 172 2917 0.04 ug/1 0.15 Spiked Amount 50.000 Recovery = 0.08% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 26130.D NP112601.M Mon Dec 03 12:10:17 2001 Page 1

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