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GCMS analysis results for sample AD26078, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD26078 conducted on December 12, 2001.

NYC-WTC_000030907–000030917

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\NOV2 001\26078.D Vial: 6 Acq On : 20 Nov 2001 5:29 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 20 18:18 2001 Quant Results File: NP103001.RES

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Nov 02 16:41:16 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.72 152 801539 ' 20.00 ug/1 0.00 19) Naphthalene-d8 15.32 136 3063983 20.00 ug/1 0.00 31) Acenaphthene-diO 20.59 164 1538904 20.00 ug/1 -0.02* 49) Phenanthrene-diO 25.02 188 2347487 20.00 ug/1 -0.02 59) Chrysene-dl2 33.06 240 1724901 20.00 ug/1 0.00 68) Perylene-dl2 37.16 264 1230797 20.00 ug/1 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.71 132 521 0.01 ug/1 0.47 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.30 152 873 0.02 ug/1 0.06 Spiked Amount 50.000 Recovery = 0.04% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.75 172 1980 0.02 ug/1 0.13 Spiked Amount 50.000 Recovery = 0.04% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2"-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.

(#) = qualifier out of range (m) = manual integration 26078.D NP103001.M Mon Dec 10 14:55:30 2001 Page 1

NYC-WTC_000030909

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NYC-WTC_000030909Source: NYC Law Department, mirrored locally

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NYC-WTC_000030679 · Box DEP Box 21

Gas chromatography-mass spectrometry scan record from late October to November 2001 regarding environmental sample analysis.

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