Gas chromatography-mass spectrometry analysis of sample AD25845, December 12, 2001, identifying other unknown compounds with threshold of 5.0 ug.
NYC-WTC_000030698–000030707Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\NOV2101\25845.D Vial: 3 Acq On : 21 Nov 2001 1:20 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 21 14:08 2001 Quant Results File: NP103001.RES
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Nov 02 16:41:16 2001 Response via : Initial Calibration DataAcq Meth : NP103001
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.71 152 886056 20.00 ug/1 -0.02 19) Naphthalene-d8 15.31 136 3386476 20.00 ug/1 -0.02 31) Acenaphthene-diO 20.59 164 1683451 20.00 ug/1 -0.02 49) Phenanthrene-diO 25.02 188 2546556 20.00 ug/1 -0.02 59) Chrysene-dl2 33.06 240 1894689 20.00 ug/1 0.00 68) Perylene-dl2 37.16 264 1353940 20.00 ug/1 0.00
System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.71 132 705 0.01 ug/1 0.47 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.28 152 880 0.02 ug/1 0.03 Spiked Amount 50.000 Recovery = 0.04% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.75 172 2166 0.02 ug/1 0.13 Spiked Amount 50.000 Recovery = 0.04% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00%
Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.
(#) = qualifier out of range (m) = manual integration 25845.D NP103001.M Mon Dec 10 15:03:30 2001 Page 1
NYC-WTC_000030700
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000030742
Laboratory report documenting GCMS analysis of sample AD25939 conducted on December 12, 2001, including surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030806
Laboratory report documenting GCMS analysis of sample AD25948 conducted on December 12, 2001, including surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030816
Laboratory report documenting GCMS analysis of sample AD25949 conducted on December 12, 2001, including surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030885
Laboratory report documenting GCMS analysis of sample AD26010 conducted on December 12, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030875
Laboratory report documenting GCMS analysis of sample AD26009 conducted on December 12, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069614
Laboratory report documenting GCMS analysis of sample AD25458 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069624
Laboratory report documenting GCMS analysis of sample AD25459 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070166
DEP laboratory report documenting GC/MS results for sample AD25843 analyzed on December 6, 2001.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069530
Laboratory report documenting GCMS analysis of sample AD25264 conducted on November 28, 2001, noting unknown compounds.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069718
Laboratory report documenting GCMS analysis of sample AD25497 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069379
Laboratory report documenting GC/MS analysis of sample AD25051 conducted on November 28, 2001.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069822
Laboratory report documenting GCMS analysis of sample AD25605 conducted on November 29, 2001, noting unknown compounds.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Gas chromatography-mass spectrometry scan record from late October to November 2001 regarding environmental sample analysis.
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NYC-WTC_000030680
Chromatogram and calibration data for DFTPP standard used to verify GC/MS instrument performance during environmental analysis.
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NYC-WTC_000030685
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NYC-WTC_000030708
Laboratory report documenting GCMS analysis of sample AD25873 conducted on December 12, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000030719
Laboratory commentary on GCMS scan of sample AD25874 dated December 13, 2001, identifying tetrachloroethane and noting a blank analysis.
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