GCMS analysis results for sample AD25945, Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\NOV2101\25945.D Vial: 11 Acq On : 21 Nov 2001 9:09 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 21 21:58 2001 Quant Results File: NP103001.RES

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Nov 02 16:41:16 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.72 152 1001079 20.00 ug/1 0.00 19) Naphthalene-d8 15.32 136 3826196 20.00 ug/1 0.00 31) Acenaphthene-dl0 20.60 164 1914345 20.00 ug/1 0.00 4 9) Phenanthrene-dl0 25.02 188 2876576 20.00 ug/1 -0.02 59) Chrysene-dl2 33.06 240 2006120 20.00 ug/1 0.00 68) Perylene-dl2 37.16 264 1392590 20.00 ug/1 0.00

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.72 132 770 0.01 ug/1 0.48 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.22 152 1290 0.03 ug/1 -0.03 Spiked Amount 50.000 Recovery 0.06% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobipheny1 18.75 172 2550 0.02 ug/1 0.13 Spiked Amount 50.000 Recovery = 0.04% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00%

Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 5.31 74 102 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chioropheno1 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3 &4-Methylphenol 0.00 108 0 N.D.

(#) = qualifier out of range (m) = manual integration 25945.D GCMS1126.M Tue Dec 11 09:03:13 2001 Page 1

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