GCMS analysis results for sample AD25940, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2101\25940.D Vial: 9 Acq On : 21 Nov 2001 7:12 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.45 0.47 ug/1 115317 1,4-Dichlorobenzene-d4 11.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone, 4 158 C9H1802 ydroxy- 3 - propyl - 062338-17-4 78 3 Oxirane, 2-me thyl-2-(1-methylethyl) 100 C6H120 072221-03-5 64 4 Methyl Isobutyl Ketone 100 C6H120 000108-10-1 58 Abundance Scan 153 (6.452 mln): 25940.D (-) m/z 43.05 1 00.00% 43

58 5000

100 6.20 6.40 6.60 6.80 * * miz-> 20 36 TT > < r. । . Thri 30 40 +5 50 ........... ............. ..

60 70 80 90 100 110 120 130 140 m/z 58.05 57.57% Abundance #63387:2-Hexanone i 43 58 — , — . 5000 6.20 6.40 6.60 6.80 100 m/z 41.00 16.67% 71 85 —mmnt —ugur " — miz-> Abundance 20 30 40 50 60 70 80 90 43 111 1 ' ■ i 100 110 120 “11968 -Hexangna 1 pdroxy-3-propyl-

58 ‘ t■11 1 I ' 1 1 1 11 1 130 140

NA 6.20 6.40 6.60 6.80 5000 29 m/z 57.00 16.53%’

71 85 100

mu, Abundance 11 ■ ■ ■' ।1111111111 ‘1 20 30 40 50 ' 11 1 • • i ■'' ■ i 1 1 ■■i■■■■i■1111111'111111'11111' 60 70 80 90 100 110 120 #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 130 140 140 • ■ । ‘ i ■ ' ■ ■ । 1 1 ' ■ । ' 43 6.20 6.40 6.60 6.80 58 m/z 100.05 14.22%

miz-> 5000

—T 20 th 30

30 40 52 50 71

J_______ ‘IT t+t 1’ 60 70 85 100 L____ -—mIIPT 611111111T 80 90 100 110 120 130 140 A, MP .20 V 6.40 6.60 6.80

25940.D NP103001.M Tue Dec 11 09:27:46 2001 Page 1

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