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GCMS calibration data, Nov 2001

Machine-extracted title · confidence 90%

Chromatogram and calibration data for DFTPP standard used to verify GC/MS instrument performance during environmental analysis.

NYC-WTC_000030680–000030684

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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Scanned page image, NYC-WTC_000030684
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\NOV2101\DFTPP.D Vial: 1 Acq On 21 Nov 2001 11:32 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D 6000000

5000000

4000000

3000000

2000000

1000000

Time-s 24.40 24.60 24.80 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 Abundance Average of 26.238 to 26.293 mln.: DFTPP.D i 400000 198

300000

200000 69 127 255 442 51 110 100000 275 224 93 0 T T 38 n'T ++ 80 100444816718012111.242. 1 . 296310323336 352365 383 403 423 T’rii rrrtitrni 01 rt f ri fi | f rt i । i i ri p i i i fl i i TITr m/z—> 40 60 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 26.238 to 26.293 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 33.0 131821 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 42.8 171304 PASS 70 69 0.00 2 0.0 57 PASS 127 198 40 60 46.3 185221 PASS ■ 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 399776 PASS 199 198 5 9 6.6 26517 PASS 275 198 10 30 19.5 78115 PASS 365 198 1 100 1.9 7446 PASS 441 443 0.01 100 94.0 32848 PASS 442 198 40 110 45.7 182586 PASS 443 442 17 23 19.1 34963 PASS

DFTPP.D NP103001.M Mon Dec 10 15:00:15 2001

NYC-WTC_000030684

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NYC-WTC_000030684Source: NYC Law Department, mirrored locally

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NYC-WTC_000030679 · Box DEP Box 21

Gas chromatography-mass spectrometry scan record from late October to November 2001 regarding environmental sample analysis.

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