GCMS method 508 calibration parameters, January 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\JAN1502\DFTPP.D Vial: 1 Acq On 15 Jan 2002 8:20 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D

3000000

2500000

2000000

1500000

1000000

500000 0 ■ 111111 f । y _ Y . A . Time-> 24.20 24.40 24.60 24.80 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 Abundance Average of 25.274 to 26.982 min.: DFTPP.D 198

6000 40

69 4000 127 442 255 110 2000 275 149 , 224

m/z-> 0 —8+ dmm, 40 60 1, 4 711 4 93 64tm r Ah 48% ril,R11/4 1 1 67 , ?4 /J ,1 n A,. . , 4, *PHRR,*fM $94 ■ “*, r ■ H 296309 323336 352365 383 403 IrfIi il j 5 'i i’i | ri r. । ‘* 1* । ।'i < i i p r 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 423

Spectrum Information: Average of 25.274 to 26.982 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 53.2 3704 PASS 68 69 0.00 2 0.0 1 PASS 69 198 0.00 100 59.9 4170 PASS 70 69 0.00 2 0.5 22 PASS 127 198 40 60 51.9 3611 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 6960 PASS 199 198 5 9 6.5 454 PASS 275 198 10 30 20.1 1397 PASS 365 198 1 100 2.3 157 PASS 441 443 0.01 100 87.9 634 PASS 442 198 40 110 54.1 3766 PASS 443 442 17 23 19.1 721 PASS

DFTPP.D GCMS1126.M Mon Feb 04 12:40:24 2002

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