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GCMS calibration data, Nov 2001

Machine-extracted title · confidence 90%

Chromatogram and calibration data for DFTPP standard used to verify GC/MS instrument performance during environmental analysis.

NYC-WTC_000030680–000030684

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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Scanned page image, NYC-WTC_000030680
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\NOV2 001\DFTPP.D Vial: 1 Acq On 20 Nov 2001 12:35 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D 5000000

4000000-

3000000

2000000

1000000

0- PA Time-> 24.40 24.60 24.80 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 Abundance Average of 26.244 to 26.281 min.: DFTPP.D 198 400000

300000

127 442 200000 69 255 51 110 100000 275 224 93 +4 /4 148.167100 121111.24,.+. 226309323336,352365, 383,403,423 „ ++ ----34 0 ‘. +1111 38 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440_

Spectrum Information: Average of 26.244 to 26.281 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 32.1 136810 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 41.6 176992 PASS 70 69 0.00 2 0.1 259 PASS 127 198 40 60 45.5 193813 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 425907 PASS 199 198 5 9 6.6 28067 PASS 275 198 10 30 20.1 85534 PASS 365 198 1 100 1.8 7837 PASS 441 443 0.01 100 94.9 37318 PASS 442 198 40 110 48.5 206709 PASS 443 442 17 23 19.0 39312 PASS

DFTPP.D NP103001.M Mon Dec 10 14:59:44 2001

NYC-WTC_000030680

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NYC-WTC_000030680Source: NYC Law Department, mirrored locally

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NYC-WTC_000030679 · Box DEP Box 21

Gas chromatography-mass spectrometry scan record from late October to November 2001 regarding environmental sample analysis.

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