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Reference standard results, sample AD25601, Nov 2001

Machine-extracted title · confidence 90%

Laboratory report of reference standard analysis for sample AD25601 conducted November 13, 2001 to validate analytical procedures.

NYC-WTC_000029552–000029557

Folder label: “525 X 10/29/01 AN 11/13 - 11/14/01

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2 Z K - O O

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O 1 C 0 0 0 Quantitation Report Quanfile: REFB1113 Quan Entries: 28 O o 0 N Comment: BOHLK: METHOD 525; INST 204; 11/13/01; REF STD “0 0 (O CH CH Sorted via: Entry Number t (S) = Standard — 0 CD 0 Cal Name of Compound S Scan# R Time Me Calc Amt(A) Units 0 O C 3 Q 3 chrysene d-12(IS) 1 1360 22:48 BB 5.000 UG/L 4 p-terphenyl d-14(IS) I 1250 20:50 VV 5.000 UG/L 5 acenaphthene d-10(SURR A 737 12:17 BB 3.681 UG/L 6 phenanthrene d-10(SURR A 1015 16:55 BU 3.772 UG/L 7 chrysene d-12 (SURR) A 1360 22:48 BB 4.430 UG/L 8 1«3-d imethy1-2-n itrobe A 478 7:58 BB 5.129 UG/L 9 triphenyl phosphate (S A 1325 22:85 BB 5.066 UG/L 10 perylene d-12 CSURR) A 1618 26:58 BB 4.360 UG/L 11 hexachlorocyclopentad i A 609 18:89 BB 3.896 UG/L 12 hexachlorobenzene A 920 15:28 BB 4.290 UG/L 13 simazine A 966 16:86 BU 4.195 UG/L 14 atrazine A 976 16:16 BB 4.762 UG/L 15 alachlor A 1103 18:23 BU 5.215 UG/L 16 bis (2-ethy Ihexy Dadipa A 1318 21:58 UU 4.460 UG/L 17 bis(2-ethyihexyl)phtha A 1378 22:58 UB 5.076 UG/L 18 benzo (a)pyrene A 1604 26:44 BB 4.067 UG/L 19 eptc A 633 18:33 BU 5.243 UG/L 20 2 j6-d in itrotoluene A 715 11:55 BB 5.505 UG/L 21 2,4-d in itrotoluene A 775 12:55 BB 4.090 UG/L 22 molinate A 783 13:83 BB 5.571 UG/L 23 terbac i1 A 1043 17:23 BB 9.937 UG/L 24 acetochlor A 1092 18:12 BU 5.624 UG/L 25 metribuzin A 1094 18:14 BU 2.668 UG/L 26 metolachlor A 1148 19:88 BU 5.567 UG/L 27 butachlor A 1222 28:22 BU 4.960 UG/L 28 4,4‘—dde A 1246 20:46 MM 5.143 UG/L

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NYC-WTC_000029556Source: NYC Law Department, mirrored locally

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NYC-WTC_000029459 · Box DEP Box 20

Gas chromatography-mass spectrometry analysis results for sample AD25458 including Hexachlorobenzene and other compounds from November 2001.

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