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Reference standard results, sample AD25601, Nov 2001

Machine-extracted title · confidence 90%

Laboratory report of reference standard analysis for sample AD25601 conducted November 13, 2001 to validate analytical procedures.

NYC-WTC_000029552–000029557

Folder label: “525 X 10/29/01 AN 11/13 - 11/14/01

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"0 I C O o o o Integration Report Quanfile: REFB1113 Quan Entries: 28 O o N Comment: BOHLK: NETHOD 525 J INST 204; 11/13/01; REF STD U O CD On C1 Sorted via: Entry Number T — 9 C1 U No Name of Compound R Time Scan# Node Peak Area Pk Height o O C 3 CD 3 chrysene d-12(IS) 22:40 1360 Auto 2,443,167 922,830 D

4 p-terphenyl d-14(IS) 20:50 1250 Auto 3,548,064 2,524,258 5 acenaphthene d-10(SURR 12:17 737 Auto 1,984,907 1,233,734 6 phenanthrene d-10(SURR 16:55 1015 Auto 3,118,947 1,311,469 7 chrysene d-12 (SURR) 22:40 1360 Auto 2,443,167 922,830 8 1,3-d imethy1-2-nitrobe 7:58 478 Auto 1,268,031 705,769 9 triphenyl phosphate (S 22:05 1325 Auto 1,774,238 745,815 10 perylene d-12 (SURR) 26:58 1618 Auto 1,285,728 249,528 11 hexach1orocyc1opentad i 10:09 609 Auto 452,714 208,921 12 hexachlorobenzene 15:20 920 Auto 1,150,814 505,487 13 simazine 16:06 966 Auto 604,777 193,575 14 atrazine 16:16 976 Auto 678,910 223,854 15 alachlor 18:23 1103 Auto 1,107,418 584,623 16 bis (2-ethyIhexy Dad ipa 21:58 1318 Auto 1,261,476 570,746 17 b is (2-ethy Ihexy l phtha 22:58 1378 Auto 4,164,315 1,687,541 18 benzo(a)pyrene 26.44 1604 Auto 1,834,701 363,988 19 eptc 10:33 633 Auto 5,003,733 3,384,925 20 2,6-d in itrotoluene 11:55 715 Auto 653,273 288,826 21 2,4-d in itrotoluene 12:55 775 Auto 727,574 259,100 22 molinate 13:03 783 Auto 2,020,727 926,168 23 terbacil 17:23 1043 Auto 923,955 318,877 24 acetochlor 18:12 1092 Auto 799,793 438,846 25 metribuzin 18:14 1094 Auto 702,547 395,321 26 metolachlor 19:08 1148 Auto 3,354,769 1,713,012 27 butachlor 20:22 1222 Auto 984,205 527,257 28 4,4'-dde 20:46 1246 Auto 1,376,252 966,379

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NYC-WTC_000029459 · Box DEP Box 20

Gas chromatography-mass spectrometry analysis results for sample AD25458 including Hexachlorobenzene and other compounds from November 2001.

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