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Reference standard results for pesticides and organics, Nov 2001

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Laboratory analysis report of reference standards used to validate pesticide and organic compound testing in sample AD25458 during November 2001.

NYC-WTC_000029505–000029509

Folder label: “525 X 10/29/01 AN 11/13 - 11/14/01

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U ।O C O O Quantitation Report Quanfile: REFA1113 Quan Entries: 28 CT o' O N. Comment: BOHLK; METHOD 525; INST 204; 11/13/01; REF STD T O CO CH O Sorted via: Entry Number 1 (S) = Standard — 9 (O 0 0 Cal Name of Compound S Scani R Time Ne Calc Amt(A) Units O C 3 CD 3 chrysene d-12(IS) l 1360 22:40 BV 5.000 UG/L S

4 p-terphenyl d-14CIS) I 1250 20:50 BB 5.000 UG/L 5 acenaphthene d-10(SURR A 737 12:17 BV 3.775 UG/L 6 phenanthrene d-10(SURR A 1015 16:55 BV 3.995 UG/L 7 chrysene d-12 (SURR) A 1360 22:40 BV 4.282 UG/L 8 1,3-d imethy1-2-n itrobe A 478 7:58 BV 4.943 UG/L 9 triphenyl phosphate (S A 1325 22:05 BB 5.607 UG/L 10 perylene d-12 (SURR) A 1617 26:57 BB 4.205 UG/L 11 hexachlorocyclopentad i A 608 10:08 BB 4.154 UG/L 12 hexachlorobenzene A 920 15:20 BB 4.297 UG/L 13 simazine A 965 16:05 BV 4.142 UG/L 14 atraz ine A 976 16:16 BB 4.793 UG/L 15 alachlor A 1103 18:23 BV 5.060 UG/L 16 bis(2-ethyihexyl)ad ipa A 1318 21:58 W 4.813 UG/L 17 b is(2-ethyIhexyl phtha A 1378 22:58 VB 8.507 UG/L 18 benzo(a)pyrene A 1603 26:43 BB 3.994 UG/L 19 eptc A 633 10:33 BV 5.040 UG/L 20 2 36-d in itrotoluene A 715 11:55 BB 5.437 UG/L 21 2,4-d in itrotoluene A 775 12:55 BB 3.755 UG/L 22 molinate A 782 13:02 BB 5.977 UG/L 23 terbacil A 1043 17:23 BV 9.116 UG/L 24 acetochlor A 1092 18:12 BV 5.631 UG/L 25 metribuzin A 1094 18:14 BV 2.875 UG/L 26 metolachlor A 1148 19:88 BB 5.551 UG/L 27 butachlor A 1222 20:22 W 4.948 UG/L 28 4,4” -dde A 1246 20:46 NN 4.666 UG/L

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NYC-WTC_000029509Source: NYC Law Department, mirrored locally

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NYC-WTC_000029459 · Box DEP Box 20

Gas chromatography-mass spectrometry analysis results for sample AD25458 including Hexachlorobenzene and other compounds from November 2001.

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