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Reference standard results for pesticides and organics, Nov 2001

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Laboratory analysis report of reference standards used to validate pesticide and organic compound testing in sample AD25458 during November 2001.

NYC-WTC_000029505–000029509

Folder label: “525 X 10/29/01 AN 11/13 - 11/14/01

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Z Z - o oK 3 o CO _s

T i C O O O O Integration Report Quanfile: REFA1113 Quan Entries: 28 CT o' N CO Comment: BOHLK: METHOD 525; INST 204; 11/13/01; REF STD o U C Sorted via: Entry Number T — O 0 CO O o No Name of Compound R Time Scan# Node Peak Area Pk Height o C 3 CD 3 chrysene d-12(I8) 22:40 1360 Auto 2,457,985 1,004,203 5

4 p-terphenyl d-14(IS) 20:50 1250 Auto 3,693,125 2,495,095 5 acenaphthene d-10(SURR 12:17 737 Auto 2,118,852 1,393,150 6 phenanthrene d-10(SURR 16:55 1015 Auto 3,437,992 1,457,607 7 chrysene d-12 (SURR) 22:40 1360 Auto 2,457,985 1,004,203 8 1,3-d imethy1-2-n itrobe 7:58 478 Auto 1,304,599 737,144 9 triphenyl phosphate (S 22:05 1325 Auto 1,975,855 806,295 10 perylene d-12 CSURR) 26:57 1617 Auto 1,247,492 250,422 11 hexachlorocyclopentad i 10:08 608 Auto 521,399 265,557 12 hexach lorobenzene 15:20 920 Auto 1,230,459 529,956 13 simazine 16:05 965 Auto 655,288 206,547 14 atrazine 16:16 976 Auto 754,281 289,761 15 alachlor 18:23 1103 Auto 1,184,481 662,019 16 bis C2-ethyIhexy DJadipa 21:58 1318 Auto 1,364,479 580,347 17 b is (2-ethy Ihexy l phtha 22:58 1378 Auto 6,601,636 2,691,130 18 benzo (a )pyrene 26:43 1603 Auto 1,816,406 339,261 19 eptc 10:33 633 Auto 5,146,901 3,652,074 20 2,6-d in itrotoluene 11:55 715 Auto 688,802 333,074 21 2,4-d in itrotoluene 12:55 775 Auto 704,185 267,600 22 mol inate 13:02 782 Auto 2,316,684 1,207,712 23 terbacil 17:23 1043 Auto 887,394 302,078 24 acetochlor 18:12 1092 Auto 882,692 498,275 25 metribuzin 18:14 1094 Auto 842,247 481,770 26 metolachlor 19:08 1148 Auto 3,687,808 1,796,559 27 butachlor 20:22 1222 Auto 1,082,807 498,164 28 4,4'-dde 20:46 1246 Auto 1,378,560 1,056,018

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NYC-WTC_000029508Source: NYC Law Department, mirrored locally

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NYC-WTC_000029459 · Box DEP Box 20

Gas chromatography-mass spectrometry analysis results for sample AD25458 including Hexachlorobenzene and other compounds from November 2001.

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