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← Document results/DEP Box 20/525 X 10/19/01 10/22/01 AN 11/3 - 11/5/01
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Spiked sample analysis for sample AD24483, Nov 2001

Machine-extracted title · confidence 85%

Results from a spiked sample test to verify recovery rates for pesticide analysis.

NYC-WTC_000028747–000028751

Folder label: “525 X 10/19/01 10/22/01 AN 11/3 - 11/5/01

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Scanned page image, NYC-WTC_000028750
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0 O I C O O O O Integration Report Quanfile: 24483MSD Quan Entries: 28 o' O N 00 Comment: BOHLK: METHOD 525; INST 204; 11/03/01; SAMPLE 24483 SPIKE DUPL “O o Sorted via: Entry Number T — o 0 O O o No Name of Compound R Time Scan# Mode Peak Area Ph Height o C 3 CD 3 chrysene d-12(IS) 22:46 1366 Auto 1,119,332 435,886 O

4 p-terphenyl d-14(IS) 28:54 1254 Auto 1,831,635 1,245,792 5 acenaphthene d-10(SURR 12:21 741 Auto 859,587 492,428 6 phenanthrene d-10(SURR 17:88 1028 Auto 1,392,834 498,663 7 chrysene d-12 (SURR) 22:46 1366 Auto 1,119,332 435,886 8 1,3-d imethy1-2-n itrobe 8:01 481 Auto 564,476 236,234 9 triphenyl phosphate (S 22:10 1338 Auto 878,676 357,232 10 perylene d-12 CSURR) 27:08 1628 Auto 667,317 112,027 11 hexachlorocyclopentad i 10:12 612 Auto 158,195 98,448 12 hexachlorobenzene 15:26 926 Auto 538,277 227,371 13 simazine 16:11 971 Auto 240,463 78,270 14 atrazine 16:22 982 Auto 326,858 125,953 15 alachlor 18:27 1187 Auto 540,628 275,645 16 bis(2-ethyIhexyl Jadipa 22:03 1323 Auto 579,356 192,795 17 bis(2-ethyIhexyl phtha 23:04 1384 Auto 2,009,195 578,896 18 benzo(a)pyrene 26:54 1614 Auto 788,122 125,979 19 eptc 10:37 637 Auto 2,725,389 1,674,481 20 2,6-d in itrotoluene 11:59 719 Auto 246,915 123,866 21 2,4-d in itrotoluene 12:59 779 Auto 272,925 91,521 22 molinate 13:06 786 Auto 917,152 426,096 23 terbacil 17:26 1846 Auto 467,310 169,567 24 acetochlor 18:16 1896 Auto 361,133 227,611 25 metribuzin 18:18 1898 Auto 389,421 217,076 26 metolachlor 19:12 1152 Auto 1,659,401 856,428 27 butachlor 20:26 1226 Auto 584,329 389,356 28 4,4'-dde 20:50 1258 Auto 537,305 280,718

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NYC-WTC_000028750Source: NYC Law Department, mirrored locally

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