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← Document results/DEP Box 20/525 X 10/25/01 AN 11/9 - 11/10/01
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Water duplicate spike analysis, 525 X, Oct-Nov 2001

Machine-extracted title · confidence 90%

Laboratory report for a duplicate spiked sample (sample AD25041) used to verify precision at the DEP laboratory.

NYC-WTC_000029219–000029223

Folder label: “525 X 10/25/01 AN 11/9 - 11/10/01

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Scanned page image, NYC-WTC_000029222
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"0 I C o o o Integration Report Quanfile: 25041MSD Quan Entries: 28 O o o N Comment: BOHLK: METHOD 525; INST 204; 11/09/01; SAMPLE 25041 MSD “0 O CD N N Sorted via: Entry Number 1 — 9 N U 0 No Name of Compound R Time Scant Node Peak Area, Pk Height O C 3 CD 3 chrysene d-1Z(IS) 22:45 1365 Auto 2,184,791 879,698 D

4 p-terphenyl d-14(IS) 20:54 1254 Auto 4,202,019 2,597,397 5 acenaphthene d-10(SURR 12:21 741 Auto 2,034,665 1,335,273 6 phenanthrene d-10(SURR 17:00 1020 Auto 3,319,287 1,400*859 7 chrysene d-12 CSURR) 22:45 1365 Auto 2,184,791 879,698 8 1,3-d imethy1-2-n itrobe 8:01 481 Auto 1,279,861 693,009 9 triphenyl phosphate (S 22:09 1329 Auto 1,537,759 528,443 10 perylene d-12 CSURR) 27:07 1627 Auto 313,883 47,332 11 hexachlorocyclopentad i 10:12 612 Auto 369,166 229,149 12 hexach lorobenzene 15:25 925 Auto 1,191,472 497,817 13 simazine 16:11 971 Auto 407,396 127,752 14 atrazine 16:22 982 Auto 741,235 266,741 15 alachlor 18:27 1107 Auto 1,288,184 818,229 16 b is (2-ethy lhexy Dadipa 22:02 1322 Auto 1,276,097 584,135 17 b is(2-ethylhexyl)phtha 23:03 1383 Auto 3,932,703 1,420,860 18 benzo(a)pyrene 26:53 1613 Auto 135,605 17,000 19 eptc 10:36 636 Auto 5,305,913 2,581,998 20 2,6-d in itrotoluene 11:59 719 Auto 595,168 244,498 21 2,4-d in itrotoluene 12:58 778 Auto 569,393 258,235 22 molinate 13:86 786 Auto 2,159,129 1,386,666 23 terbacil 17:27 1047 Auto 909,319 295,991 24 acetochlor 18:16 1096 Auto 847,343 476,639 25 metribuzin 18:18 1098 Auto 572,661 299,890 26 metolachlor 19:12 1152 Auto 3,810,235 2,218,363 27 butachlor 20:26 1226 Auto 1,112,477 725,581 28 4,4'-dde 20:49 1249 Auto 1,340,470 987,068

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NYC-WTC_000029222Source: NYC Law Department, mirrored locally

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Department of Environmental Protection laboratory record from late October to early November 2001 regarding sample tracking.

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NYC-WTC_000029152 · Box DEP Box 20

Gas chromatography-mass spectrometry analysis results for sample AD25041 including DDT and Endrin data from November 2001.

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