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Spiked sample analysis sample AD24481, October 2001

Machine-extracted title · confidence 70%

Spiked quality control sample analysis for AD24481 completed 10/31/01 measuring recovery of pesticides and organic compounds added to verify analytical method performance.

NYC-WTC_000028566–000028570

Folder label: “525 X 10/17/01 AN 10/31 - 11/1/01

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Scanned page image, NYC-WTC_000028569
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z z oK oK 3 o t _s

"0 1 C o O o Integration Report Quanfile: 24481MS Quan Entries: 28 O o o N Comment: BOHLK: METHOD 525; INST 204; 10/31/01; SAMPLE 24481 MS “0 o 00 CH Sorted via: Entry Number 1 — CD CD 9 oo No Name of Compound R Time Scan# Node Peak Area Pk Height O C 3 CD 3 chrysene d-12(IS) 22:50 1370 Auto 985,115 366,513 D

4 p-terphenyl d-14(IS) 20:57 1257 Auto 2,633,430 1,754,062 5 acenaphthene d-10(SURR 12:26 746 Auto 853,723 451,758 6 phenanthrene d-10(SURR 17:07 1027 Auto 1,374,906 472,454 7 chrysene d-12 (SURR) 22:50 1370 Auto 985,115 366,513 8 1,3-d imethy 1-2-n itrobe 8:06 486 Auto 531,391 262,295 9 triphenyl phosphate (S 22:13 1333 Auto 777,626 258,186 10 perylene d-12 (SURR) 27:18 1638 Auto 607,468 105,062 11 hexachlorocyclopentad i 10:16 616 Auto 136,011 64,248 12 hexachlorobenzene 15:33 933 Auto 580,991 244,377 13 simazine 16:19 979 Auto 43,394 10,682 14 atrazine 16:30 990 Auto 240,091 71,916 15 alachlor 18:32 1112 Auto 536,314 256,595 16 b is (2-ethy Ihexy Dadipa 22:06 1326 Auto 1,053,495 327,837 17 b is (2-ethy Ihexy l phtha 23:08 1388 Auto 1,800,267 532,170 18 benzo(a)pyrene 27:04 1624 Auto 772,974 124,128 19 eptc 10:41 641 Auto 2,497,253 1,521,608 20 2,6-d in itrotoluene 12:03 723 Auto 254,128 95,539 21 2»4-d in itrotoluene 13:03 783 Auto 278,422 76,120 22 molinate 13:11 791 Auto 909,808 527,245 23 terbacil 17:31 1051 Auto 44,993 11,950 24 acetochlor 18:20 1100 Auto 362,682 192,655 25 metribuzin 18:22 1102 Auto 197,786 77,424 26 metolachlor 19:16 1156 Auto 1,549,334 879,580 27 butachlor 20:29 1229 Auto 465,813 321,634 28 4,4'-dde 20:52 1252 Auto 534,256 372,278

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NYC-WTC_000028569Source: NYC Law Department, mirrored locally

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