GCMS calibration results for sample AE10812, May 2002

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020521\0521C1.D Vial-: 2 Acq On : 21 May 2002 8:58 am Operator: Nefliu Sample : ccv Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 21 10:00 2002 Quant Results File: SCAN020521.RES Method : C:\MSDCHEM\1\METHODS\M020523.M (RTE Integrator) Title : Method 616 Methoprene Last Update : Fri May 24 08:58:56 2002 Response via : Initial Calibration Abundance TIC: 0521 C1.D 2200000

2000000 N v 1800000 o 4 1 g % s I2 1600000 s 1 z J £ 2c 2 I a C1

1400000 e 1 b 8 1200000 1S 1000000 2 I 800000 2 2 fi. 0 0

2 2f 2 6 2d

h 5 to

g l8 J I I pt 0 § 2 ! iiii88 I fl l 10 O

i EN : § a gB g § 600000 0 2 i c I 3 § & 0 g f? o a 0 if 2 89)2 2Z &ss 5 g 8 53 I I i o o CD 8 4 & C 20 8(Q t 25 8a $8 CD E 400000 t 0% g g I" I 8 o" 2 & 8 82 cE6 O o Q TO 200000 1 S &of8 Z o 1 N o 5 fl LO t — LO

...... 1.1.. i o — Q 0 ■ ■ I 1 ' ■ ■ i ' ’ r ' 1 1 —4 y o Time—> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00 42.00 44.00 46.00 oTO I 0 o

o 0521C1.D M020523.M Fri May 24 09:09:10 2002 Page 3 5d o > 2 2