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GCMS calibration results for sample AE10812, May 2002

Machine-extracted title · confidence 100%

Laboratory report of GCMS calibration data showing response values and detection limits for 15 volatile organic compounds on May 17-21, 2002.

NYC-WTC_000025508–000025511

Folder label: “GCMS X 5/17/02 A 5/16/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020521\0521Cl.D Vial: 2 Acq On : 21 May 2002 8:58 am Operator: Nefliu Sample : ccv Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 21 09:59:10 2002 Quant Results File: SCAN020521.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 21 08:15:50 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoranthene 36.05 202 422849 9.92 ug/1 98 3 9) Pyrene 36.65 202 409975 10.14 ug/1 97 40) Buthylbenzylphthalate 38.93 149 167206 8.74 ug/1 99 41) Benz(a)anthracene 39.91 228 337579 9.56 ug/1 99 42) Chrysene 39.99 228 336828 10.09 ug/1 96 43) Bis(2-ethylhexyl)phthalate 40.52 149 220419 9.28 ug/1 97 45) Di-n-Octyl phthalate 42.03 149 303079m 8.08 ug/1 46) Benzo(b)fluoranthene 42.37 252 246586m 9.29 ug/1 47) Benzo(k)fluoranthene 42.43 252 298338 10.20 ug/1 99 48) Benzo(a)pyrene 43.02 252 243444 9.54 ug/1 97 49) Indeno(1,2,3-cd)pyrene 45.22 276 124513m 7.65 ug/1 5 0) Dibenz(a,h)anthracene 45.32 278 137380m 8.81 ug/1 51) Benzo(ghi)perylene 45.76 276 156305 9.67 ug/1 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0521C1.D M020523.M Fri May 24 09:09:09 2002 Page 2

NYC-WTC_000025510

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NYC-WTC_000025510Source: NYC Law Department, mirrored locally

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