GC-MS chromatogram data, sample 11410, May 2002

2 < Quantitation Report (QT Reviewed) - o o CD 2o Data File : C:\MSDCHEM\l\DATA\051702\0515REFl.D Acq On : 18 May 2002 2:38 am Vial: Operator: 17 Mclean — O I Sample : 5/15 eh Inst : Instrumen C O o o Mise Multiplr: 1.00 o' o o N MS Integration Params: EVENTS.E “0 o CH N Quant Time: May 21 11:59 2002 Quant Results File: 050102.RES — 0 o O Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) o Q Title : 508 Modified GC/MS scan C 3 Last Update : Mon May 13 11:40:29 2002 CD Response via : Initial Calibration Abundance TIC:0515REF1.D o 2600000 It O z§ 2400000 CQ g § s 2 J82 c 2200000 sf 1s g CM 8§ j 6 G N 2000000 & g e 2

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Time-> 00——-1 , 4.00 6.00 -N 8.00 10.00 — 12.00 T

14.00 r —r 16.00 i.n, 18.00 , mil 20.00 22.00 24.00 26.00 28.00 30.00 L 32.00 V T 34.00 ' 1 I 1 7 36.00 38.00 Tdl

0515REF1.D 050102.M Tue May 21 15:59:21 2002 Page 3