GCMS reference analysis results, sample AE11379, May 21 2002

2 z Quantitation Report (QT Reviewed) - K O o 3 Data File : C:\MSDCHEM\1\DATA\051702\0515REF2.D Acq On : 18 May 2002 3:27 am Vial: Operator: 18 Mclean CD — o "0 1 Sample : 5/15 eh Inst : Instrumen C o O o Mise o Multiplr: 1.00 o' o "0 N CH MS Integration Params: EVENTS.E o o Quant Time: May 21 12:00 2002 Quant Results File: 050102.RES — 00 0 O Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) o Q C Title : 508 Modified GC/MS scan 3 Last Update : Mon May 13 11:40:29 2002 CD

Response via : Initial Calibration Abundance TIC: 0515REF2.D

3200000 o

3000000 o y I§ CO d2 g 2800000- I I1 I E

Iz c

2600000 jJ a2 CM

8 5 2 8 2400000

2200000 I 6s c o 2000000 §Q z N

1800000

3 2aI qo d B 2 g I 8 i 1 62 1 8 0 1600000 11 i 8 g

i 11 ® o Bo g 2g” c 2 & 8 1400000

1200000 .[lu 188 a

111 igk9® 8 S8

55 1 2Q 5 CM

2 85 1 gc i i I 9 cc

tg R I(

I g52 3 g 1000000 8852 Ns e ! Jo I s 8i -2 Q£e— 20 Ov C

t X CM 76

&8&o 800000 2 1$ g 6 g o I of 8 st 600000 £ CM’ C

2 5 400000 j f Q C

200000

0 4.00 I I 6.00 TT L— I -T —— 26.00 ' ' 28.00 ' ' 30.00 ' ' 32.00 TT 1—r Time-> 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 34.00 36.00 38.00

0515REF2.D 050102.M Tue May 21 12:00:45 2002 Page 3