GCMS analysis results for sample AE11383, May 22 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\11382.D Vial: 9 Acq On : 17 May 2002 7:18 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 3-Oxetanol, 2,2,3-trimethyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.35 ug/L 320150 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Quad

1 3-Oxetanol, 2,2,3-trimethyl- 116 C6H1202 025910-96-7 23 2 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 3 2-Hexanone, 5-methyl- 114 C7H140 000110-12-3 9 4 2-Propanone, 1-(1-methylethoxy)- 116 C6H1202 042781/12-4 9 Abundance Scan 791 (7.727 min): 11382.D (-782) (-) | m/z 43.10 100.00% 43

5000 58 87 ■ ■ । 1 1 1 1 । 1 ■ ■ ■ । 1 ■ ■ ■ । 98 7.40 7.60 7.80 8.00

miz-> 0- 20 30 37, h 40 -4414 50 —— 70 60 ■ i । 80 । ■ 90 tv ,!........................... 100 110 120 m/z 58.05 29.51% __ Abundance #5761:3-Oxetanol, 2,2,3-trimethyl- 43 M/WWww 5000 58 7.40 7.60 7.80 8.00 29 71 86 m/z 87.00 22.16% I. . 38, 53, 1 65 n/z-> 01 21 1.......... 20 30 40 4.’’I ■ ' 1 ‘ i 1 ■ 50 60 70 80 81— 90 98 100 1 1 i ■ ■ ■ 1 i r ' ■ ' i 1 110 120 Abundance #4163: 3-Pyrrolidinol 43

7.40 7.60 7.80 8.00 5000 m/z 41.10 13.37% 87 57 68 0- 1 i 1 1 ' 1 i ■ ■ ■ ■ r +5211—177,82 m/z-> Abundance 20 30 40

43 50 60 70 80 #109705: 2-Hexanone, 5-methyl- 90 100 110 120 AAAAAAAALMAMAAA 7.40 7.60 7.80 8.00 m/z 83.0.0 12.49%

5000 58 27

m/z-> 0 4 - ll ' ' 20 30 40 50 60 71 । ■ ■ i ' ■ ■ 70 ■ i ■ ■ 80 85 99 ■ ■ i ■ ■ ■ ■' i ■ ' > ' I ' 90 100 110 114 i ' । i ' 120 7.40 7.60 7.80 8.00

11382.D 050102.M Tue May 21 11:54:18 2002 Page 6

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