Laboratory report showing GC/MS analysis results for sample AE10816 including surrogate recovery data on May 14, 2002.
NYC-WTC_000023502–000023516Folder label: “GCMS X 5/9/02 A 5/13/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\051302\10816.D Vial: 13 Acq On : 13 May 2002 9:16 pm ■ Operator: Mclean Sample : 5/9 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 3-Oxetanol, 2,2,3-trimethyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 7.73 0.36 ug/L 328178 1,4-Dichlorobenzene-d4 9.94
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Oxetanol, 2,2,3-trimethyl- 116 C6H12O2 025910-96-7 23. 2 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 22 3 4-Hexen-2-one 98 C6H10O 025659-22-7 12 4 2-Pentanone, 3-methylene- 98 C6H10O 004359-77-7 10 Abundance Scan 791 (7.727 min): 10816.D (-787) (-) m/z 43.10 100.00% 43
5000 58 I "Wyw 87 98 ' 4 1 1 * ’ ■ 1 ‘ * 1 • 1
m/z-> 0 -H+RA— 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 . ... 11,111.,.. M m/z 7.40 7.60 58.10 7.80 8.00 29.38% Abundance #5761:3-Oxetanol, 2,2,3-trimethyl- 43 wyWwwk 5000 58 7.40 7.60 7.80 8.00 29 71 m/z 87.00 18.51% 86
mfz-> 0 21. .. .1 H 3+4—65++ 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 81 ,| 98 HTT " i' "' Ih " i" " i"1' i' ■" i' ‘ " i
Abundance #110033: 4-Penten-2-one, 4-methyl- 43 1 ' 1 1 1 11 I 7,40 7.60 7.80 8.00 5000 m/z 98.10 14.99%
28 83 55 98
/z-> 0 LL I,... 1,1111.।।।।. 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ■ i" ■ ■ i" “ i"111" " ।" i
Abundance #7570:4-Hexen-2-one ■ ■ i 1 ' ' ■ । 43 7.40 7.60 7.80 8.00 m/z 59.10 12.51% 1 5000
55 98 29 , 50 ., — 62 67 77 83 0 1 . I | I I I I | I ITT-ItI t I | | ! I . | |II 1 | "" | I . 11 | . i . । . .. . । TTTTI . > , . . . . | . > I . , . . .. | r. । Tp-r ■•i111111"' I 1I Tl/Z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.40 7.60 7.80 8.00
10816.D 050102.M Tue May 14 11:43:01 2002 Page 7
NYC-WTC_000023513
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NYC-WTC_000023531
Laboratory report page showing GC/MS analysis for sample AE10850 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022886
GCMS analytical report for environmental sample AE09332 including surrogate compound data from May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022916
Laboratory report documenting GCMS analysis of environmental sample AE09568 conducted on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024153
Document noting low recovery in GCMS scan of sample AE10205 and subsequent re-extraction yielding 85% recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025479
Laboratory report documenting GCMS analysis of sample AE11423 conducted on May 30, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023487
Laboratory report showing GC/MS analysis results for sample AE10164 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022938
Laboratory report documenting GCMS analysis of environmental sample AE09569 conducted on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025371
Laboratory report of GCMS analysis for sample AE11417 conducted on May 30, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023439
Laboratory report showing GC/MS analysis results for sample AE10137 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025447
Laboratory report showing GCMS results for sample AE11421 analyzed on May 30, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022795
GCMS analytical report for environmental sample AE09151 including surrogate compound data from May 15, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025414
Laboratory report documenting GCMS analysis of sample AE11419 conducted on May 30, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000023405
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
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NYC-WTC_000023406
Log sheet recording drip rates, volumes, and pH measurements during liquid-liquid extraction procedures for environmental samples in May 2002.
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Laboratory report showing non-detect results for volatile organic compounds in a method blank sample AE10137 analyzed on May 14, 2002.
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Laboratory report showing GC/MS calibration data for volatile organic compounds in sample AE10137 analyzed on May 14, 2002.
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Laboratory report showing GC/MS scan data for deuterated surrogate compounds in sample CAL10 analyzed on May 13-14, 2002.
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