GCMS analysis results for sample AE11381, May 22 2002

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Data File : C:\MSDCHEM\1\DATA\051702\11380.D Vial : 7 Acq On : 17 May 2002 5:40 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 3-Oxetanol, 2,2,3-trimethyl- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.31 ug/L 279451 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Oxetanol, 2,2,3-trimethyl- 116 C6H12O2 025910-96-7 40/ 2 3-Pyrrolidinol 87 C4H9NO 040499-83-0 25 3 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 17 4 2-Amino-octadec-7-ene-l,3-diol m... 323 C19H38BN02 1000143-52-/ 12 Abundance Scan 791 (7.727 min): 11380.D (-785) (-) m/z 43.10 100.00% 43 __

5000 58 87 98 7.40 7.60 7.80 8.00 Ok . . . ]/ Ill 1 >- " i1" 11 “ ।' i11 69 ■ j 1111111111 111 [ । > 111' 1111111 m/z 58.10 30.21% r111141111 ' i" ■' i H r1" । m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #5761: 3-Oxetanol, 2,2,3-trimethyl- 43 MMMMW "MWAWAs 5000 58 1 ' I 1 1 ‘ ‘ 1 1 1 • i 1 ' ' ■ i 7.40 7.60 7.80 8.00 29 71 m/ z 87.10 18.51%

0 ............. 38,1 +th53+4—5++ TTmptt 81 + 98 86 " • i"1 ■ i" ■ ■ 111" I I /z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #4163: 3-Pyrrolidinol 43 -----

7.40 7.60 7.80 8.00 5000 m/z 59.10 13.99% 87 57 68 77 82. TTTTTTH opanonpomanpomoaponsst Ot '" l1'' ‘ I'' ‘11" " I'''' l'''' I miz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #110033: 4-Penten-2-one, 4-methyl- 43 7.40 7.60 7.80 8.00 m/z 55.10 10.15% 5000 83 55 98

m/z-> 0 - 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 L i'1" i U 7.40 7.60 7.80 8.00

11380.D 050102.M Mon May 20 15:46:46 2002 Page 7

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