GCMS calibration verification for sample AE11379, May 20, 2002

Quantitation Report (QT Reviewed) Data File C:\MSDCHEM\1\DATA\0 52 0 0 2\CAL8 0.D Vial: 3 Acq On 20 May 2002 12:16 pm Operator: Mclean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 20 15:11 2002 Quant Results File: 050102.RES Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 13 11:40:29 2002 Response via : Initial Calibration Abundance TIC: CAL80.D

5000000

4500000 iO 2 o 2o 16 a « o 2 4000000 & S 6 o2 22 3500000 2o is g8 c 8 eg 8I g i65 !

I ?g g 28 I % I N

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3000000 88 8 § 85 22 2 95 ad 8 85 g •3 Jo 5 C fl 2 o § § L 3 28 o & 388 Qo s o g i§8 1" s “ C c c

58 CD

111 2500000 Frisi c

2000000 S F s s s 8$ A c g I 2 0)

fS 2

J s 18 s 88 8 8 5 0 (r

12 & f. 'I N of + N 0 2

if 1500000 I 88 s £ &

C CD E 3 1000000 1 O o Q 3 500000 00 co t o o LO CXI Q o — <J 1 TIT -- o o o Time-s 4.00 6.00 ' 8.00 1000 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 o o 0- 1 o oo CAL80.D 050102.M Mon May 20 15:12:07 2002 Page 3 1d > > 7 7