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GCMS calibration verification for sample AE11379, May 20, 2002

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Laboratory report documenting GCMS calibration verification for sample AE11379 conducted on May 20, 2002, listing specific compound concentrations.

NYC-WTC_000025076–000025079

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document quantltatlon Report (Ql Reviewed)

Data File C:\MSDCHEM\1\DATA\0 5 2 0 0 2\CAL8 0.D Vial: 3 Acq On 20 May 2002 12 :16 pm Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 20 15:09:31 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 13 11:40:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.55 202 28599347 72.56 ug/L 99 38) Pyrene 27.19 202 27692663 77.30 ug/L 98 39) Butylbenzylphthalate 29.53 149 12094088 75.75 ug/L # 97 40) Benzo(a)anthracene 30.79 228 22211537 77.86 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.39 149 16133482 74.77 ug/L 96 42) Chrysene 30.89 228 22759536m 77.06 ug/L 44) Di-n-octylphthalate 33.24 149 21987064m 83.31 ug/L 45) Benzo(b)fluoranthene 33.76 252 19441371 89.81 ug/L 98 46) Benzo(k)fluoranthene 33.84 252 21720644 79.85 ug/L 98 47) Benzo(a)pyrene 34.57 252 18117212m 83.85 ug/L 48) Indeno(1,2,3-cd)pyrene 37.41 276 13212694 87.23 ug/L 100 49) Dibenz(a,h)anthracene 37.53 278 14027060 87.07 ug/L 99 50) Benzo(g,h,i)perylene 38.16 276 13413377m 79.31 ug/L

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL80.D 050102.M Mon May 20 15:12:06 2002 Page 2

NYC-WTC_000025077

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NYC-WTC_000025077Source: NYC Law Department, mirrored locally

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