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GCMS blank analysis results for sample AE11379, May 21, 2002

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Laboratory report showing GCMS blank analysis for sample AE11379 conducted on May 21, 2002, with results below minimum reporting levels.

NYC-WTC_000025054–000025071

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\051702\0515LB.D Vial: 16 Acq On : 18 May 2002 1:49 am Operator: Mclean Sample : 5/15 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98. L *********** ********************************************************** Peak Number 10 Stannane, tributylethyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 39.75 0.99 ug/L 676139 Perylene-dl2 34.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Stannane, tributylethyl- 320 C14H32Sn 019411-60-0 14 2 Benzaldehyde,(diphenylmethyliden ... 284 C20H16N2 1000148-58-8 $ 3 Naphthalene, l-chloro-2,6-dimeth... 222 C12H11C1O2 025315-09-7 JI 4 IH-Pyrrolo[2,3-c]pyridine-3-prop... 222 C11H14N2O3 032682-61-45 Abundance Scan 6241 (39.749 min): 0515LB.D (-6239) (-) m/z 222.05 100400% 149 222 296 36 430 73 5000

355 01 191 i li 267 _____ I ‘I’ .. I I 39.40 m/ Z 149.00 39.60 39.80 99.62% miz- > 50 100 150 200 250 300 350 400 Abundance #126475: Stannane, tributylethyl- 207 121 , 151 177 5000 Trl 29 263 39.40 39.60 39.80 235 291 m/z 147.05 93.92 % 0- 56 1 r-, 79, { d.dI, Al i , 1 —— h /z-> 50 100 150 200 250 '300 350 400 Abundance #97685: Benzaldehyde,(diphenylmethylidene)hydrazone 207 284 77 103 / YW W 180 39.40 39.60 39.80 5000 m/z 296.10 72.62%

0 L mfe-> 50 100 150 200 250 300 350 400 Abundance #88163: Naphthalene, 1-chloro-2,6-dimethoxy- 222 39.40 39.60 39.80 179 m/z 207.00 66.54% 5000 136 nlaoww m/z-> 0 12.5 75 113 157 50 1 1 * 4 11 -4— 100 150 200 250 300 350 400 39,40 39.60 39.80

0515LB.D 050102.M Tue May 21 11:58:30 2002 Page 13

NYC-WTC_000025070

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NYC-WTC_000025070Source: NYC Law Department, mirrored locally

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