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GCMS analysis results for sample AE11377, May 28, 2002

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Laboratory report documenting GCMS analysis of sample AE11377 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000025022–000025030

Folder label: “GCMS X 5/14/02 A 5/21/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2102\11310.D Vial: 24 Acq On : 21 May 2002 11:26 pm Operator: Sample : EXTRACTS/14 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

8.11 21.87 ug/1 1581030 1,4-Dichlorobenzene-d4 12.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 72 2 Acetone 58 C3H60 000067-64-1 9 3 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 4 2,3/-Butanedione, monooxime 101 C4H7NO2 000057-71-6 7 Abundance ' Scan 335 (8.110 min): 11310.D (-) m/ z 43.05 100.00% 4|3 I 5000 59 . — 1 । ■ 1 ■ ' । 101 7.80 8.00 8.20 8.40 -3444 tmtT 53 , 69 83 mj m/z-> Abundance I"" I'1"I 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 #64274:2-Pentanone, 4-hydroxy-4-methyl- 43 ‘11131111"111111111111"11‘1‘71111T m/ z 59.10 n 36.48%

5000 59 7.80 8.00 8.20 8.40 m/z 58.10 17.58% 27 101 49 83 r ■" ।1 ■11J ■" ।11 "T mlimeipl +TTTTTTH Tm-r-r THT m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62322: Acetone 43 11111/"11/*.1/1//1/d/d/"//"/t/1///"/"/T 7.80 8.00 8.20 8.40 5000 m/Z 101.15 11.26% 58 27 m I I I I |-|L l | I I ! ! | I > I I I I I ................ "I" 11" " r 1" i " " i" '' i" ■' i" ‘' i1"111"1111111" " 111' m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #1448: CH2=CHCH2C(O)OCH3 1 ' ' i r ' ' ■ i 1 r' ■ i 1 1 i ' ■ 1 ' i 43 7.80 8.00 8.20 8.40 m/z 41.15 6.77% 5000

58 I" "I""I 38 4 +TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTWTTPTTTTTTTTTTTTT I 72 100 T , IP I I ITT | I I T I | m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 7.80 8.00 8.20 8.40

11310.D GCMS0520.M Wed May 22 09:21:44 2002 Page 1

NYC-WTC_000025029

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NYC-WTC_000025029Source: NYC Law Department, mirrored locally

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