NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\MAY2102\LBB.D Vial: 17
Acq On : 21 May 2002 4:33 pm Operator:
Sample : EXTRACTS/14 Inst : 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
8.11 23.83 ug/1 1519490 1,4-Dichlorobenzene-d4 12.15
Hit# of Tentative ID MW MolForm CAS# Qual
1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 40
2 Acetone 58 C3H60 000067-64-1 9
3 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9
4 2,3-Butanedione, monooxime________ 101 C4H7NO2 000057-71-6 7
Abundance Scan 335 (8.113 min): LBB.D (-) m/z 43.05 100.00%
43
5000
59
1 1 ' i ■ ' ■ r i ■ f' ' i ' ■ 1 1 i ■ ■ ' ■ i
101 7.80 8.00 8.20 8.40
. ........................................ 53 69 77 83 |
t+ I 1 1 r ■ i ' ■ ■ ' i 1 '' 1 1 1 1 ' 1 1 I' 1 1 1 1 1 m/z 59.10 32.57%
m/z-> 10 20 30 40 50 60 70 80 90 100 110
Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl-
43
___________________ _ _________
5000 ' ' 1 ' I ' ' 1 ' ITOE" । . “TT i | I I I I |
59 7.80 8.00 8.20 8.40
m/z 58.10 19.25%
15 31 101
83 ।
—1* ,4411 . . । । i TT 1 ‘1 I । । । rr— । । । । । t-| । । । । । ।
m/z-> 10 20 30 40 50 60 70 80 90 100 110
Abundance #62322: Acetone
43
1
7.80 8.00 8.20 8.40
5000 m/z 101.15 9.99%
58
27
4 1-r-TT-. i ' 1 1 ■ i ' ■ 1 ■ । 1 1 ■ r । 1 1 1 1 i 1 1 1 1 i 1
miz—> 10 20 30 40 50 60 70 80 90 100 110
Abundance #1448: CH2=CHCH2C(O)OCH3
‘ ' i ' ' ' ' i 1 ' ' ' I ' i ' ' 1 ' I
43 7.80 8.00 8.20 8.40
m/z 41.05 5.85%
5000
58
........ ................. 72I ■ ■ - i 100
1 1 i ' ■ i ■ ■ 1 ■ i ■ ■ ' 1 r1 141111-1/1
■ ■ ।
PI11 1 I r -------
m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40
LBB.D GCMS0520.M Wed May 22 09:22:30 2002 Page 1
NYC-WTC_000024963
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