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GCMS analysis results for sample AE10302, May 10, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10302 conducted on May 10, 2002, including surrogate recovery data.

NYC-WTC_000024946–000024952

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document yuantltatlon Report (V1 Reviewed) Data File : C:\MSDCHEM\l\DATA\020509\10302.D Vial: 27 Acq On : 10 May 2002 12:19 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 10 13:30:10 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator Title : Method 508 GC/MS Scan ' Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 519085 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1974298 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 1050894 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1741874 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1329632 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 892461 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.53 207 49782 5.93 ug/1 -0.04 Spiked Amount 10.000 Recovery = 59.30% Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10302.D SCAN020507.M Tue May 14 14:21:56 2002 Page 1

NYC-WTC_000024946

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NYC-WTC_000024946Source: NYC Law Department, mirrored locally

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