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GCMS analysis results for sample AE10247, May 28, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10247 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024907–000024914

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020509\10247.D Vial: 25 Acq On : 10 May 2002 10:21 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 10 11:33:41 2002 Quant Results File: SCANO20507.RB

Quant Method Title : : C:\MSDCHEM\1\METHODS\SCAN020507.M Method 508 GC/MS Scan (RTE Integrator) VY JX Last Update Response via DataAcq Meth

Internal Standards : : : Thu May 09 09:21:01 2002 Initial Calibration 508SCAN1

R.T. Qlon Response Cone Units Dev(Min) r 1) 1,4-Dichlorobenzene-d4 11.37 152 501270 40.00 ug/1 -0.02 10) Naphthalene-d8 16.53 136 1926184 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 1017257 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1752399 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1421952 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 883156 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.54 207 41382 5.09 ug/1 -0.04 Spiked Amount 10.000 Recovery = 50.90%

Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10247.D SCAN020507.M Tue May 14 14:19:45 2002 Page 1

NYC-WTC_000024907

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NYC-WTC_000024907Source: NYC Law Department, mirrored locally

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