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GCMS quantitation results for sample AE10301, May 2002

Machine-extracted title · confidence 90%

Laboratory report of GCMS analysis for sample AE10301 conducted on May 28, 2002.

NYC-WTC_000024915–000024926

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020516\10301.D Vial: 24 Acq On : 17 May 2002 8:04 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 17 10:50:16 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 16 14:49:15 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 300196 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1120188 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.45 164 596441 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.71 188 995208 40.00 ug/1 -0.03 38) Chrysene-dl2 39.92 240 750004 40.00 ug/1 -0.06 44) Perylene-dl2 43.15 264 458527 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.55 207 161831 33.97 ug/1 -0.02 Spiked Amount 40.000 Recovery 84.92% Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10301.D SCAN020507.M Fri May 17 10:51:12 2002 Page 1

NYC-WTC_000024917

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NYC-WTC_000024917Source: NYC Law Department, mirrored locally

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