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GCMS analysis results for sample AE10243, May 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10243 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024824–000024831

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020509\10243.D Vial: 21 Acq On : 10 May 2002 6:23 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 10 08:29:47 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Itegratof Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 562481 40.00 ug/1 -0.01 10) Naphthalene-d8 16.54 136 2141603 40.00 ug/1 -0.03 17) Acenaphthene-diO 24.46 164 1144068 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1948652 40.00 ug/1 -0.02 38) Chrysene-dl2 39.94 240 1609388 40.00 ug/1 -0.05 44) Perylene-dl2 43.16 264 1019860 40.00 ug/1 -0.02

System Monitoring Compounds 27) TCMX 27.54 207 56410 6.17 ug/1 -0.03 Spiked Amount 10.000 Recovery = 61.70%

Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10243.D SCAN020507.M Tue May 14 14:14:53 2002 Page 1

NYC-WTC_000024824

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NYC-WTC_000024824Source: NYC Law Department, mirrored locally

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